Solid Phase Extraction Preconcentration and HPLC Determination of Biogenic Amines Using A Hydrazone Derivative Immobilized on Sol-Gel Matrix
الكلمات المفتاحية:
Hydrazone، biogenic amine، Sol-gel، extractionالملخص
A sorbent material based on a hydrazone ligand, formaldehyde-2,4–dinitrophenylhydrazone was prepared by immobilizing the ligand into a silica sol-gel matrix. The capability of the sorbent material for the extraction of seven biogenic amines was investigated. Under the optimum condition, the sorbent material exhibited preferential selectivity towards the aliphatic (putrescine, PUT; cadaverine, CAD; spermidine, SPD) and the heterocyclic (histamine, HIS) over the aromatic (tryptamine, TRY; 2-phenylethylamine, PEA, tyramine, TYR) biogenic amines.
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